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Patent · US11413570B2 · B2 · US

Rotary bed sorption system including recycled isolation loop and purge/regeneration loop

(11) Publication number
US11413570B2
(21) Application number
16/459,228
(22) Filing date
2019-07-01
(30) Priority date
2018-06-29
(43) Publication date
2022-08-16
(45) Date of grant
2022-08-16
(51) IPC
B01D 53/06; B01D 53/26; B01D 53/02
(52) CPC
  • B01D Separation: 53/06, 2257/404, 2257/708, 2257/80, 2258/06, 2259/4009, 53/002, 53/261, 53/265
(73) Assignee
Munters Corp
(72) Inventors
Douglas S. Jefferson; Stephen C. Brickley
(54) Title
Rotary bed sorption system including recycled isolation loop and purge/regeneration loop
(57) Abstract

A rotary sorption bed system includes a rotating sorbent mass of a regenerable sorbent material, in a cycle of operation, a given volume of the sorbent mass sequentially passing through first, second, third, fourth, and fifth zones, before returning to the first zone; a process fluid stream directed through the first zone; a regeneration fluid stream directed through the third zone; and an isolation fluid stream that recirculates in a closed loop independent of the process fluid stream and the regeneration fluid stream through the second and fourth zones. The regeneration fluid stream passes through the fifth zone before passing through the third zone.

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Claims (13)

  1. A method of reducing the sorbate concentration of a process fluid stream using a sorption bed system comprising a rotating mass of a regenerable sorbent material, the method comprising the steps of: rotating the sorbent mass so that, in a cycle of operation, a given volume of the sorbent mass sequentially passes through first, second, third, fourth, and fifth zones, before returning to the first zone; passing a process fluid stream through the sorbent mass in the first zone; passing a regeneration fluid stream through the sorbent mass in the third zone; and recycling an isolation fluid stream in a closed loop, independent of the process fluid stream and the regeneration fluid stream, between the sorbent mass in the fourth zone and in the second zone, wherein the regeneration fluid stream passes through the fifth zone before passing through the third zone.
  2. The method of claim 1, wherein the direction of fluid flow in each of the first, fourth, and fifth zones is the same.
  3. The method of claim 2, wherein the direction of fluid flow in each of the second and third zones is the same.
  4. The method of claim 3, wherein the direction of fluid flow in each of the first, fourth, and fifth zones is opposite the direction of fluid flow in each of the second and third zones.
  5. The method of claim 1, wherein a concentration of at least one member selected from the group consisting of water vapor, volatile organic compounds, and nitrous oxides is reduced as a result of passing the process fluid stream through the sorbent mass in the first zone.
  6. The method of claim 1, further comprising the steps of: recirculating the regeneration fluid stream in a closed loop by first passing the regeneration fluid stream through the fifth zone; and heating the regeneration fluid stream after exiting the fifth zone and prior to passing the regeneration fluid stream through the third zone.
  7. The method of claim 1, further comprising the step of recirculating the process fluid stream in a substantially closed loop to dehydrate or maintain dryness of a product.
  8. A rotary sorption bed system, comprising: a rotating sorbent mass of a regenerable sorbent material, in a cycle of operation, a given volume of the sorbent mass sequentially passes through first, second, third, fourth, and fifth zones, before returning to the first zone; a process fluid stream directed through the first zone; a regeneration fluid stream directed through the third zone; and an isolation fluid stream that recirculates in a closed loop independent of the process fluid stream and the regeneration fluid stream through the second and fourth zones, wherein the regeneration fluid stream passes through the fifth zone before passing through the third zone.
  9. The system of claim 8, wherein the process fluid stream and the regeneration fluid stream are passed through the sorbent mass in opposite directions, and the isolation fluid stream is passed through the sorbent mass in the same direction as a fluid stream immediately following the isolation fluid stream with respect to the direction of rotation of the sorbent mass.
  10. The system of claim 8, further comprising a heating device disposed in the regeneration fluid stream between the fifth zone and the third zone so as to further heat the regeneration fluid stream before passing through the third zone.
  11. The system of claim 8, wherein the process fluid stream is at a higher pressure than the regeneration fluid stream.
  12. The system of claim 8, wherein the process fluid stream is at a lower pressure than the regeneration fluid stream.
  13. The system of claim 8, wherein the process fluid stream is recirculated in a substantially closed loop to dehydrate or maintain dryness of a product.

Description

This application claims the benefit of provisional U.S. patent application Ser. No. 62/691,919, filed Jun. 29, 2018, which is incorporated herein by reference.

The present invention relates generally to a rotary bed sorption system, and, in particular, to a rotary bed sorption system that includes both a recycled isolation loop and a purge/regeneration loop. The invention also relates to methods of designing and operating such a system.

Rotary bed sorption systems have long been used to collect a sorbate from one fluid stream, sometimes called a process or sorption fluid stream, and transfer it, in a more concentrated form, to a second fluid stream, sometimes called a desorption or regeneration fluid stream. Commonly-removed sorbates include water vapor, volatile organic compounds (“VOCs”), nitrous oxides (“NOx”), and the like.

It is important in a rotary bed sorption system, particularly one in which a low sorbate concentration is desired in the treated fluid, to minimize any cross-contamination between the process fluid stream and the regeneration fluid stream. Contamination can result from pressure differences in the fluid streams themselves, or vapor pressure differences within the matrix of the rotating sorbent disk.

Another source of possible contamination lies in areas of the sorbent disk that are adjacent to the active sorptive area, but that do not see active fluid flow during the cycle. Usually these are the areas at the center and outer periphery of the sorbent disk that are covered by sealing systems.

Citations (12)

  • US4701189A
  • US4775484A
  • US5802870A
  • US6328787B1
  • US20050235827A1
  • US7101414B2
  • US8628608B2
  • US20090139254A1
  • US20100275775A1
  • US20120152116A1
  • US20120204718A1
  • WO2012109550A1
Record as JSON
{
  "publication_number": "US11413570B2",
  "country": "US",
  "kind": "B2",
  "title": "Rotary bed sorption system including recycled isolation loop and purge/regeneration loop",
  "abstract": "A rotary sorption bed system includes a rotating sorbent mass of a regenerable sorbent material, in a cycle of operation, a given volume of the sorbent mass sequentially passing through first, second, third, fourth, and fifth zones, before returning to the first zone; a process fluid stream directed through the first zone; a regeneration fluid stream directed through the third zone; and an isolation fluid stream that recirculates in a closed loop independent of the process fluid stream and the regeneration fluid stream through the second and fourth zones. The regeneration fluid stream passes through the fifth zone before passing through the third zone.",
  "claims": [
    "1. A method of reducing the sorbate concentration of a process fluid stream using a sorption bed system comprising a rotating mass of a regenerable sorbent material, the method comprising the steps of: rotating the sorbent mass so that, in a cycle of operation, a given volume of the sorbent mass sequentially passes through first, second, third, fourth, and fifth zones, before returning to the first zone; passing a process fluid stream through the sorbent mass in the first zone; passing a regeneration fluid stream through the sorbent mass in the third zone; and recycling an isolation fluid stream in a closed loop, independent of the process fluid stream and the regeneration fluid stream, between the sorbent mass in the fourth zone and in the second zone, wherein the regeneration fluid stream passes through the fifth zone before passing through the third zone.",
    "2. The method of claim 1, wherein the direction of fluid flow in each of the first, fourth, and fifth zones is the same.",
    "3. The method of claim 2, wherein the direction of fluid flow in each of the second and third zones is the same.",
    "4. The method of claim 3, wherein the direction of fluid flow in each of the first, fourth, and fifth zones is opposite the direction of fluid flow in each of the second and third zones.",
    "5. The method of claim 1, wherein a concentration of at least one member selected from the group consisting of water vapor, volatile organic compounds, and nitrous oxides is reduced as a result of passing the process fluid stream through the sorbent mass in the first zone.",
    "6. The method of claim 1, further comprising the steps of: recirculating the regeneration fluid stream in a closed loop by first passing the regeneration fluid stream through the fifth zone; and heating the regeneration fluid stream after exiting the fifth zone and prior to passing the regeneration fluid stream through the third zone.",
    "7. The method of claim 1, further comprising the step of recirculating the process fluid stream in a substantially closed loop to dehydrate or maintain dryness of a product.",
    "8. A rotary sorption bed system, comprising: a rotating sorbent mass of a regenerable sorbent material, in a cycle of operation, a given volume of the sorbent mass sequentially passes through first, second, third, fourth, and fifth zones, before returning to the first zone; a process fluid stream directed through the first zone; a regeneration fluid stream directed through the third zone; and an isolation fluid stream that recirculates in a closed loop independent of the process fluid stream and the regeneration fluid stream through the second and fourth zones, wherein the regeneration fluid stream passes through the fifth zone before passing through the third zone.",
    "9. The system of claim 8, wherein the process fluid stream and the regeneration fluid stream are passed through the sorbent mass in opposite directions, and the isolation fluid stream is passed through the sorbent mass in the same direction as a fluid stream immediately following the isolation fluid stream with respect to the direction of rotation of the sorbent mass.",
    "10. The system of claim 8, further comprising a heating device disposed in the regeneration fluid stream between the fifth zone and the third zone so as to further heat the regeneration fluid stream before passing through the third zone.",
    "11. The system of claim 8, wherein the process fluid stream is at a higher pressure than the regeneration fluid stream.",
    "12. The system of claim 8, wherein the process fluid stream is at a lower pressure than the regeneration fluid stream.",
    "13. The system of claim 8, wherein the process fluid stream is recirculated in a substantially closed loop to dehydrate or maintain dryness of a product."
  ],
  "description_excerpt": "This application claims the benefit of provisional U.S. patent application Ser. No. 62/691,919, filed Jun. 29, 2018, which is incorporated herein by reference.\n\nThe present invention relates generally to a rotary bed sorption system, and, in particular, to a rotary bed sorption system that includes both a recycled isolation loop and a purge/regeneration loop. The invention also relates to methods of designing and operating such a system.\n\nRotary bed sorption systems have long been used to collect a sorbate from one fluid stream, sometimes called a process or sorption fluid stream, and transfer it, in a more concentrated form, to a second fluid stream, sometimes called a desorption or regeneration fluid stream. Commonly-removed sorbates include water vapor, volatile organic compounds (“VOCs”), nitrous oxides (“NOx”), and the like.\n\nIt is important in a rotary bed sorption system, particularly one in which a low sorbate concentration is desired in the treated fluid, to minimize any cross-contamination between the process fluid stream and the regeneration fluid stream. Contamination can result from pressure differences in the fluid streams themselves, or vapor pressure differences within the matrix of the rotating sorbent disk.\n\nAnother source of possible contamination lies in areas of the sorbent disk that are adjacent to the active sorptive area, but that do not see active fluid flow during the cycle. Usually these are the areas at the center and outer periphery of the sorbent disk that are covered by sealing systems.",
  "cpc": [
    "B01D 53/06",
    "B01D 2257/404",
    "B01D 2257/708",
    "B01D 2257/80",
    "B01D 2258/06",
    "B01D 2259/4009",
    "B01D 53/002",
    "B01D 53/261",
    "B01D 53/265"
  ],
  "ipc": [
    "B01D 53/06",
    "B01D 53/26",
    "B01D 53/02"
  ],
  "assignees": [
    "Munters Corp"
  ],
  "inventors": [
    "Douglas S. Jefferson",
    "Stephen C. Brickley"
  ],
  "filing_date": "2019-07-01",
  "publication_date": "2022-08-16",
  "grant_date": "2022-08-16",
  "priority_date": "2018-06-29",
  "application_number": "US-201916459228-A",
  "family_id": "68985817",
  "cited_by_count": 6,
  "citations": [
    "US4701189A",
    "US4775484A",
    "US5802870A",
    "US6328787B1",
    "US20050235827A1",
    "US7101414B2",
    "US8628608B2",
    "US20090139254A1",
    "US20100275775A1",
    "US20120152116A1",
    "US20120204718A1",
    "WO2012109550A1"
  ]
}

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