Flashline heater system and method

{
  "publication_number": "US10301404B2",
  "country": "US",
  "kind": "B2",
  "title": "Flashline heater system and method",
  "abstract": "The present embodiments provide a system and method for separation within a polymer production process. Specifically, a flashline heater configured according to present embodiments may provide more time than is required for complete vaporization of liquid hydrocarbons that are not entrained within a polymer fluff produced within a polymerization reactor. Such extra time may allow for liquid hydrocarbons that are entrained within the polymer fluff to be vaporized.",
  "claims": [
    "1. A method, comprising: polymerizing an olefin monomer in a reactor using an olefin polymerization catalyst to generate a polymer slurry, wherein the polymer slurry includes polymer fluff and liquid; receiving a discharge stream from the reactor in a flashline heater, wherein the discharge stream comprises the polymer fluff, the liquid, and a vapor, wherein the flashline heater comprises a plurality of segments, a first segment of the plurality of segments is configured to receive the discharge stream from the reactor, and a second segment of the plurality of segments is configured to direct the discharge stream toward a separation vessel; and heating the discharge stream in the flashline heater using a heating medium, such that the polymer fluff, the liquid, and the vapor are in thermal equilibrium in the second segment of the plurality of segments, wherein heating the discharge stream in the flashline heater using the heating medium comprises selectively adjusting a flow of the heating medium to one or more segments of the plurality of segments based on a temperature of the discharge stream within the second segment of the plurality of segments.",
    "2. The method of claim 1, wherein heating the discharge stream in the flashline heater using the heating medium comprises directing the heating medium through an outer conduit of one or more segments of the plurality of segments of the flashline heater and flowing the discharge stream in an inner conduit of the flashline heater to place the heating medium in thermal communication with the discharge stream.",
    "3. The method of claim 1, wherein selectively adjusting the flow of the heating medium to the one or more segments of the plurality of segments based on the temperature of the discharge stream within the second segment comprises directing the flow of the heating medium into the first segment of the plurality of segments and blocking the flow of the heating medium into the second segment of the plurality of segments.",
    "4. The method of claim 1, wherein selectively adjusting the flow of the heating medium to the one or more segments of the plurality of segments based on the temperature of the discharge stream within the second segment comprises directing the flow of the heating medium into every three segments of the plurality of segments.",
    "5. The method of claim 1, wherein selectively adjusting the flow of the heating medium to the one or more segments of the plurality of segments based on the temperature of the discharge stream within the second segment comprises directing the flow of the heating medium into a first set of segments of the plurality of segments and blocking the flow of the heating medium into a second set of segments of the plurality of segments, wherein the first set of segments is upstream of the second set of segments with respect to a flow of the discharge stream through the flashline heater.",
    "6. The method of claim 1, comprising directing the heating medium to the one or more segments of the plurality of segments of the flashline heater from a cooling jacket of the reactor.",
    "7. The method of claim 1, wherein a temperature difference between the polymer fluff and the vapor exiting the second segment of the plurality of segments of the flashline heater is less than 1° F.",
    "8. The method of claim 1, wherein heating the discharge stream in the flashline heater using the heating medium comprises directing the discharge stream through the flashline heater for at least 8 seconds.",
    "9. The method of claim 1, comprising generating polyolefin pellets from the polymer fluff stream downstream of the separation vessel.",
    "10. A method, comprising: receiving a discharge stream comprising a polymer slurry from a polymerization reactor in a flashline heater, wherein the flashline heater comprises a plurality of segments, a first segment of the plurality of segments is configured to receive the discharge stream from the polymerization reactor, a second segment of the plurality of segments is configured to direct the discharge stream toward a separation vessel, and wherein the polymer slurry comprises a liquid, a vapor, and polymer fluff; heating the discharge stream in the flashline heater using a heating medium, such that at least 75% of the liquid, including liquid entrained within the polymer fluff, vaporizes, and wherein the polymer fluff, the liquid, and the vapor are substantially in thermal equilibrium with one another in the second segment; and selectively adjusting a flow of the heating medium to one or more segments of the plurality of segments based on a temperature of the discharge stream within the second segment of the plurality of segments.",
    "11. The method of claim 10, wherein heating the discharge stream in the flashline heater using the heating medium comprises heating the discharge stream to a temperature below a melting point of the polymer fluff.",
    "12. The method of claim 10, wherein heating the discharge stream in the flashline heater using the heating medium comprises heating the discharge stream to a temperature between 178° F. and 182° F.",
    "13. The method of claim 10, comprising heating the discharge stream in the flashline heater using the heating medium, such that at least 98% of the liquid, including liquid entrained within the polymer fluff, vaporizes.",
    "14. The method of claim 10, wherein heating the discharge stream in the flashline heater using the heating medium comprises directing the discharge stream through the flashline heater for at least 8 seconds.",
    "15. The method of claim 10, wherein a temperature difference between the polymer fluff and the vapor exiting the second segment of the plurality of segments of the flashline heater is less than 1° F.",
    "16. The method of claim 10, comprising generating polyolefin pellets from the polymer fluff downstream of the separation vessel.",
    "17. A system, comprising: a flashline heater comprising a plurality of segments, wherein a first segment of the plurality of segments is configured to receive a discharge stream from a polymerization reactor and a second segment of the plurality of segments is configured to direct the discharge stream toward a separation vessel, wherein the discharge stream comprises a solid part, a liquid part, and a vapor part; a source of a heating medium fluidly coupled to each segment of the plurality of segments, wherein the heating medium flowing through one or more segments of the plurality of segments is configured to transfer thermal energy to the discharge stream to place the vapor part, the liquid part, and the solid part in thermal equilibrium in the second segment of the plurality of segments; a plurality of valves configured to adjust a flow of the heating medium to the plurality of segments; and a controller operatively coupled to the plurality of valves, wherein the controller is configured to selectively direct the heating medium from the source of the heating medium to the one or more segments of the plurality of segments based on a temperature of the discharge stream within the second segment of the plurality of segments.",
    "18. The system of claim 17, wherein a first diameter of the first segment of the plurality of segments is different than a second diameter of the second segment of the plurality of segments.",
    "19. The system of claim 17, wherein a first length of the first segment of the plurality of segments is different than a second length of the second segment of the plurality of segments.",
    "20. The system of claim 17, wherein a valve of the plurality of valves is configured to adjust a flow of the heating medium to multiple segments of the plurality of segments."
  ],
  "description_excerpt": "The present disclosure relates generally to polymer production and, more specifically, to removing diluent from slurry discharged from a polymerization reactor.\n\nThis section is intended to introduce the reader to aspects of art that may be related to aspects of the present approaches, which are described and/or claimed below. This discussion is believed to be helpful in providing the reader with background information to facilitate a better understanding of the various aspects of the embodiments described herein. Accordingly, it should be understood that these statements are to be read in this light, and not as admissions of prior art.\n\nAs chemical and petrochemical technologies have advanced, the products of these technologies have become increasingly prevalent in society. In particular, as techniques for bonding simple molecular building blocks into longer chains (or polymers) have advanced, the polymer products, typically in the form of various plastics, have been increasingly incorporated into various everyday items. For example, polyolefin polymers, such as polyethylene, polypropylene, and their copolymers, are used for retail and pharmaceutical packaging, food and beverage packaging (such as juice and soda bottles), household containers (such as pails and boxes), household items (such as appliances, furniture, carpeting, and toys), automobile components, pipes, conduits, and various industrial products.",
  "cpc": [
    "C08F 110/02",
    "B01D 1/04",
    "B01D 1/24",
    "B01J 19/06",
    "B01J 19/1837",
    "B01J 2219/00006",
    "B01J 8/005",
    "C08F 10/00",
    "C08F 2/00",
    "C08F 2/14",
    "C08F 6/003",
    "C08L 23/00"
  ],
  "ipc": [
    "B01D 1/04",
    "B01J 19/18",
    "B01J 8/00",
    "C08F 110/02",
    "C08F 6/00",
    "B01D 1/24",
    "B01J 19/00",
    "B01J 19/06",
    "C08F 10/00"
  ],
  "assignees": [
    "Chevron Phillips Chemical Co LP"
  ],
  "inventors": [
    "John D. Hottovy",
    "Scott E. Kufeld"
  ],
  "filing_date": "2018-03-01",
  "publication_date": "2019-05-28",
  "grant_date": "2019-05-28",
  "priority_date": "2011-06-30",
  "application_number": "US-201815909621-A",
  "family_id": "46545883",
  "cited_by_count": 4,
  "citations": [
    "US2825721A",
    "US3195613A",
    "US3248179A",
    "GB991089A",
    "US3167113A",
    "US3234994A",
    "US3290278A",
    "US4022580A",
    "US4136061A",
    "US4126743A",
    "US4184036A",
    "GB2028836A",
    "US4211863A",
    "US4424341A",
    "GB2157701A",
    "US4654801A",
    "US4676870A",
    "US4900498A",
    "US5183866A",
    "US5565175A",
    "US5575979A",
    "US5597892A",
    "US5207929A",
    "US5387659A",
    "US6042790A",
    "US5411925A",
    "US6005061A",
    "US5624877A",
    "US5648439A",
    "US5565174A",
    "US5455314A",
    "US5965675A",
    "US5708082A",
    "US6815511B2",
    "US6806324B2",
    "US7033545B2",
    "US20040136881A1",
    "US20040192860A1",
    "US6743869B2",
    "US6239235B1",
    "US6114501A",
    "US6800698B2",
    "US6926868B2",
    "US6281300B1",
    "US6833415B2",
    "US6319997B1",
    "US6380325B1",
    "US6204344B1",
    "WO1999047251A1",
    "US6858682B2",
    "EP1344563A2",
    "US6670431B2",
    "US7034090B2",
    "US6045661A",
    "US6051631A",
    "US7005485B2",
    "US6967230B2",
    "US20040230031A1",
    "US6239300B1",
    "US6559247B2",
    "US6262191B1",
    "WO2000053306A1",
    "US6239225B1",
    "US6420497B1",
    "US20030109651A1",
    "US20010039329A1",
    "US20040198927A1",
    "US6723804B1",
    "US7179426B2",
    "US20040116625A1",
    "US7015289B2",
    "US7524904B2",
    "US20050186126A1",
    "US6838531B2",
    "US7087685B2",
    "US6953553B2",
    "US6818186B2",
    "US20040116597A1",
    "US6908971B2",
    "US7736597B2",
    "US20060159595A1",
    "US7014821B2",
    "WO2004031245A1",
    "EP1415999A1",
    "US7106437B2",
    "US6753387B1",
    "US20090228259A1",
    "US20050091021A1",
    "US20050095176A1",
    "US7037980B2",
    "US20090037027A1",
    "US7417095B2",
    "US7315369B2",
    "US7433761B2",
    "US7400941B2",
    "US7531606B2",
    "US7517947B2",
    "US7109290B2",
    "US7759457B2",
    "US7741430B2",
    "US7645841B2",
    "US20060045823A1",
    "US20060063896A1",
    "US20060100399A1",
    "US7781546B2",
    "US7572866B2",
    "US7505127B2",
    "US7505129B2",
    "US20070078238A1",
    "US7615596B2",
    "US7547750B2",
    "US20070142576A1",
    "US7718732B2",
    "EP1860126A1",
    "US7957947B2",
    "US7964699B2",
    "US7943727B2",
    "WO2008052943A1",
    "EP1918308A1",
    "US20090164046A1",
    "US20110166313A1",
    "US20110028684A1",
    "US7750095B2",
    "US20100056732A1",
    "US20100056707A1",
    "US7999044B2",
    "US20100322836A1",
    "US20130005929A1",
    "US20140121334A1",
    "US8871886B1"
  ]
}